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The acid insoluble fraction should contain the original, pristine sample, minus the carbonate contaminants, if the acid wash has had its desired effect.It is placed in a petrie dish or beaker and dried in an oven prior to combustion or further pretreatment.
Many samples from terrestrial environments, such as wood, charcoal and peat, will often contain small amounts of absorbed carbonates from percolating groundwater.
This material is non-contemporaneous and must be removed.
The samples most often given solvent pretreatments such as this are wood, soil organics, peat and charcoal, from specific environments.
A variety of solvents may be used in the extraction process, depending on the type of material and the contaminants present.
The insoluble fraction usually contains the sample minus the contaminant and is the dateable component.
Sometimes, samples undergo a solvent extraction prior to ABA pretreatment to remove contaminants such as resins and waxes.After approximately one hour it is removed and placed into a buchner funnel.The buchner apparatus uses the pressure of flowing water to create a vacuum.It is then rinsed in a buchner funnel with distilled water to reduce the p H levels towards neutral.Following this, the sample is immersed in a 5% diluted, boiling Na OH solution for approximately one hour, after which it is rinsed or centrifuged again.A soxhlet extractor is the most common apparatus used in the extraction method.Tags: Adult Dating, affair dating, sex dating